Sunday, August 03, 2025

x̄ - > Nanoimprint Lithography: Statistical Modeling

Nanoimprint Lithography: Statistical Modeling

An elegant interplay of engineering precision and scientific control. This is a perfect entry into statistical modeling and control in nanoimprint lithography or microfabrication.

πŸ“ Top-Level Overview

Top Panel (Cross-section & DoE Pattern)

  • Si stamp with cavities and protrusions presses into a PMMA polymer.
  • The patterned grid suggests a Design of Experiments (DoE) layout.

Bottom Panel (3D Topography)

  • Likely obtained from AFM or profilometry.
  • Height data shows feature fidelity and pattern replication.

πŸ“Š Statistical Modeling & Process Control

πŸ”§ 1. Process Characterization

Use Design of Experiments to vary parameters like temperature, pressure, and time. Model outputs such as fidelity, roughness, and height.

πŸ“‰ 2. Response Surface Methodology (RSM)


Y = Ξ²₀ + Σβₖ Xβ‚– + Σβₖₖ Xβ‚–² + Σβₖₗ Xβ‚– Xβ‚— + Ξ΅
  

Where Y is the output, Xi are input factors, and Ξ΅ is error.

πŸ“ 3. Statistical Process Control (SPC)

Use control charts to monitor process drift or anomalies (e.g., ̄X and R-charts).

🧠 4. Machine Learning

  • PCA for dimension reduction
  • Random Forests / SVM for defect classification
  • Gaussian Processes for complex predictions

πŸŽ“ Summary

  • Physical process ✓
  • Statistical design ✓
  • Modeled equations ✓
  • SPC tools ✓
  • Machine learning ✓

πŸ”§ Step 1: Define the Process

We model the PMMA embossing process. The response variable is feature height (ΞΌm).

VariableSymbolUnitsLevels
Embossing PressureX1MPa5, 10, 15
Embossing TemperatureX2°C120, 140, 160
Holding TimeX3sec30, 60, 90

πŸ“€ Step 2: Experimental Design

We apply a Central Composite Design (CCD), reducing the 27 runs to 19 using factorial, axial, and center points.

πŸ“Š Step 3: Simulated Data


Y = 0.5 + 0.05X1 + 0.03X2 + 0.02X3 - 0.0005X1X2 + 0.0003X1² + Ξ΅
Ξ΅ ~ N(0, 0.05²)
  

Here are the first 10 simulated data points:

RunPressure (MPa)Temp (°C)Time (s)Height (ΞΌm)
15.00120.030.04.68
25.00120.090.05.85
35.00160.030.05.79
45.00160.090.07.03
515.00120.030.04.61
615.00120.090.05.81
715.00160.030.05.60
815.00160.090.06.76
918.41140.060.05.61
101.59140.060.05.90

πŸ” Regression Model


Height = 0.529 + 0.022X1 + 0.030X2 + 0.020X3 - 0.0004X1X2 + 0.0012X1²
  

R² = 0.997 → nearly perfect fit.

Significant Terms: Temperature, Time, Interaction (X1*X2), Pressure²

Would you like to visualize the surface, monitor with SPC charts, or export the dataset and code?

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